Synthesis and Magnetic Properties of Maghemite (γ-Fe2O3) Short-Nanotubes

نویسندگان

  • W Wu
  • XH Xiao
  • SF Zhang
  • TC Peng
  • J Zhou
  • F Ren
  • CZ Jiang
چکیده

We report a rational synthesis of maghemite (gamma-Fe(2)O(3)) short-nanotubes (SNTs) by a convenient hydrothermal method and subsequent annealing process. The structure, shape, and magnetic properties of the SNTs were investigated. Room-temperature and low-temperature magnetic measurements show that the as-fabricated gamma-Fe(2)O(3) SNTs are ferromagnetic, and its coercivity is nonzero when the temperature above blocking temperature (T(B)). The hysteresis loop was operated to show that the magnetic properties of gamma-Fe(2)O(3) SNTs are strongly influenced by the morphology of the crystal. The unique magnetic behaviors were interpreted by the competition of the demagnetization energy of quasi-one-dimensional nanostructures and the magnetocrystalline anisotropy energy of particles in SNTs.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Synthesis and characterization of magnetic γ- Fe2O3 nanoparticles: Thermal cooling enhancement in a sinusoidal headbox

Nano-size maghemite (γ-Fe2O3) particles were prepared in one step using ultrasound radiation. The obtained nanoparticles were characterized by SEM, TEM , XRD, FTIR, and VSM. The results revealed that the synthesized nanoparticles were spherical, mono-dispersed and uniform. Furthermore, the crystalline structure of nanoparticles endorsed by X-ray diffraction study. The FTIR spectra have provided...

متن کامل

Improve Synthesis of Iron Oxide Nanorode with Hydrothermal Method

Maghemite and magnetite nanoparticles and nanorode are now losing interests in the field of nanobiotechnology and pharmaceutical for their applications. This paper reports on a hydrothermal process for the synthesis of Fe2 O3 in the γ-phases nanorodes, when the hydrothermal temperature was 100 ̊ C. The uniqueness of the method lies in the use of ferrous ammonium sulphate, hexamine was added as t...

متن کامل

γ-Fe2O3@KSF: A recyclable catalyst for the efficient synthesis of pyrano-pyrimidinone derivatives

In this work, γ-Fe2O3@KSF as a stable heterogeneous and magnetic catalyst was prepared by the successive coating of γ-Fe2O3 shell on KSF core. The prepared reagent was characterized using different methods including FT-IR, XRD, TGA and SEM techniques and used for the one-pot synthesis of pyrano-pyrimidinone derivatives. All reactions were performed under mild conditions, during short reaction t...

متن کامل

Hybrid magnetic iron oxide nanoparticles with tunable field-directed self-assembly.

We describe the synthesis of hybrid magnetic ellipsoidal nanoparticles that consist of a mixture of two different iron oxide phases, hematite (α-Fe2O3) and maghemite (γ-Fe2O3), and characterize their magnetic field-driven self-assembly. We demonstrate that the relative amount of the two phases can be adjusted in a continuous way by varying the reaction time during the synthesis, leading to stro...

متن کامل

Synthesis of benzimidazole derivatives using Ni2+ supported on hydroxyapatite-core@shell γ-Fe2O3 nanoparticles both under solvent and solvent-free conditions

Ni2+ supported on hydroxyapatite-core@shell γ-Fe2O3 nanoparticles (γ-Fe2O3@HAp-Ni2+) was found to be a useful catalyst for the synthesis of benzimidazole derivatives from o-phenylenediamine and aldehydes under solvent and solvent-free conditions at 80 °C. This reaction affords the corresponding benzimidazole derivatives compared with the classical reactions this method consistently gives a high...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره 5  شماره 

صفحات  -

تاریخ انتشار 2010